Chopped sample heating for quantitative profile analysis of low energy electron diffraction spots at high temperatures

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Kury, P.; Zahl, P.; Horn-von Hoegen, M.; Voges, C.; Frischat, H. et al.: Chopped sample heating for quantitative profile analysis of low energy electron diffraction spots at high temperatures. In: Review of Scientific Instruments 75 (2004), Nr. 11, S. 4911-4915. DOI: https://doi.org/10.1063/1.1807003

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Sum total of downloads: 166




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Abstract: 
Spot profile analysis low energy electron diffraction (SPA-LEED) is one of the most versatile and powerful methods for the determination of the structure and morphology of surfaces even at elevated temperatures. In setups where the sample is heated directly by an electric current, the resolution of the diffraction images at higher temperatures can be heavily degraded due to the inhomogeneous electric and magnetic fields around the sample. Here we present an easily applicable modification of the common data acquisition hardware of the SPA-LEED, which enables the system to work in a pulsed heating mode: Instead of heating the sample with a constant current, a square wave is used and electron counting is only performed when the current through the sample vanishes. Thus, undistorted diffration images can be acquired at high temperatures. © 2004 American Institute of Physics.
License of this version: Es gilt deutsches Urheberrecht. Das Dokument darf zum eigenen Gebrauch kostenfrei genutzt, aber nicht im Internet bereitgestellt oder an Außenstehende weitergegeben werden.
Document Type: Article
Publishing status: publishedVersion
Issue Date: 2004
Appears in Collections:Fakultät für Mathematik und Physik

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pos. country downloads
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1 image of flag of Germany Germany 96 57.83%
2 image of flag of United States United States 21 12.65%
3 image of flag of China China 12 7.23%
4 image of flag of Russian Federation Russian Federation 5 3.01%
5 image of flag of Czech Republic Czech Republic 5 3.01%
6 image of flag of No geo information available No geo information available 4 2.41%
7 image of flag of Taiwan Taiwan 4 2.41%
8 image of flag of France France 4 2.41%
9 image of flag of Vietnam Vietnam 2 1.20%
10 image of flag of United Kingdom United Kingdom 2 1.20%
    other countries 11 6.63%

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